HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 12361632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | N-(2-Hydroxyethyl)imidazole | HCID 74168 | — |
| Product | HCID 12361632 | HCID 12361632 | 85.1% |
Reaction Steps
In a nitrogen atmosphere, a mixture of 112 g of 2-(1H-imidazol-1-yl)ethanol, synthesized in Synthesis Example 1, and 122 g of acetic anhydride was stirred at room temperature for 16 hours. The reaction mixture was subjected to conventional aqueous work-up and then purified by vacuum distillation, obtaining 131 g of 2-(1H-imidazol-1-yl)ethyl acetate (boiling point 102° C./27 Pa, yield 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141351B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-6badd93e79964396b50b92c4e72e94b2 |
| Source note | uspto-grants-2006_11 |