Glycidyl methacrylate → Butyl Acrylate

HRID 723287Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 723287
[C:1]([O:6][CH2:7][CH:8]1O[CH2:9]1)(=[O:5])[C:2]([CH3:4])=C.[CH3:11]OC1C=CC(O)=CC=1>[Br-].C([N+](CCCC)(CCCC)CCCC)CCC>[C:1]([O:6][CH2:7][CH2:8][CH2:9][CH3:11])(=[O:5])[CH:2]=[CH2:4]

Komponenten

4

Edukt 2

HCID 7837Glycidyl methacrylate2×HCID 90154-Methoxyphenol

Produkt 1

HCID 8846Butyl Acrylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 74236Tetrabutylammonium BromideKatalysator

Versuchsvorschrift

After the completion of the reaction, the solution was cooled to room temperature. To the solution, 15 g of glycidyl methacrylate, 0.5 g of p-methoxyphenol and 1.5 g of tetrabutylammonium bromide were added. The mixture was stirred until these added compounds dissolved completely. The solution thus obtained was heated to 80° C., and an addition reaction was allowed to take place for 16 hours between the carboxyl group in the copolymer and the epoxy group in the glycidyl methacrylate. Thereafter, the solution was cooled to room temperature to obtain an alkali soluble resin (A-5) in the form of resin solution.

Aufarbeitung

  1. customAfter the completion of the reaction
  2. dissolutiondissolved completely
  3. customThe solution thus obtained
  4. temperaturewas heated to 80° C.
  5. additionan addition reaction
  6. customfor 16 hours
  7. temperatureThereafter, the solution was cooled to room temperature
  8. customto obtain an alkali soluble resin (A-5) in the form of resin solution

Quellen und Nachweise

ORD-Eintrag
ord-1aed0f691a62417fb559b18f29719391
Quelldatensatz
uspto-grants-2006_11
Patentnummer
US07141355B2

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