HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 723297Generated: October 30, 2026
Methyl Acrylate → HCID 21872624, compound
https://huagongshe.com/reaction/723297
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 2-Phenylbenzimidazole | HCID 12855 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21872624 | HCID 21872624 | 60% |
Reaction Steps
A mixture of 194 g of 2-phenylbenzimidazole, 103 g of methyl acrylate and 500 g of methanol was heated and stirred at 60° C. for 100 hours. The solvent was distilled off in vacuo, followed by purification by column chromatography. There was obtained methyl 3-(2-phenyl-1H-benzimidazol-1-yl)-propionate (yield 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07141352B2 |
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| Source dataset | uspto-grants-2006_11 |
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| ORD ID | ord-86344f3c682b4fe2bdd97f1a0120b530 |
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| Source note | uspto-grants-2006_11 |
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