HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21873334, compound → HCID 21873414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21873334 | HCID 21873334 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21873414 | HCID 21873414 | — |
Reaction Steps
Palladium(II) hydroxide (20% on carbon, 0.5 g) was added to a solution of (4-benzyloxyphenyl)-(2,2-dimethoxyethyl)amine (3.5 g) in ethanol (50 mL) under nitrogen. The nitrogen atmosphere was replaced by hydrogen and the mixture was shaken for 3 hours. The catalyst was filtered off and the filtrate was concentrated. The crude product was reacted further without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141561B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-29d335d8b56e4ccebe5dece31cb7f01a |
| Source note | uspto-grants-2006_11 |