HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylamino)ethanol → 2-(Methyl(4-nitrophenyl)amino)ethan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylamino)ethanol | HCID 8016 | — |
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(Methyl(4-nitrophenyl)amino)ethan-1-ol | HCID 4547077 | — |
Reaction Steps
A mixture of 4-fluoronitrobenzene (20 g) and 2-methylaminoethanol (56 mL) was left to stand for 12 hours and then diluted with ethyl acetate. It was washed with water. The organic phase was dried and concentrated. The product with the molecular weight of 196.21 (C9H12N2O3);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141561B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-d4179862f6084027901ef93b149140d5 |
| Source note | uspto-grants-2006_11 |