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HRID723358

反应详情

EQUATION

反应方程式

HRID 723358 的结构方程式

REACTANTS

反应物

2
结构：CNCCO
HCID8016

N-Methyl-N-hydroxyethylamine

C3H9NO

结构：O=[N+]([O-])c1ccc(F)cc1
HCID9590

1-Fluoro-4-nitrobenzene

C6H4FNO2

PRODUCTS

生成物

1
结构：CN(CCO)c1ccc([N+](=O)[O-])cc1
HCID4547077

2-(Methyl(4-nitrophenyl)amino)ethanol

C9H12N2O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

A mixture of 4-fluoronitrobenzene (20 g) and 2-methylaminoethanol (56 mL) was left to stand for 12 hours and then diluted with ethyl acetate. It was washed with water. The organic phase was dried and concentrated. The product with the molecular weight of 196.21 (C9H12N2O3);

WORKUP

后处理

  1. waitwas left
  2. washIt was washed with water
  3. customThe organic phase was dried
  4. concentrationconcentrated