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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 723359Generated: October 30, 2026

HCID 9888078, compound → HCID 21873392, compound

https://huagongshe.com/reaction/723359

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9888078HCID 9888078—
ReactantHCID 178418361HCID 178418361—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
ProductHCID 21873392HCID 21873392—

Reaction Steps

Palladium(II) hydroxide (20 mg) was added to a solution of 1-(4-(2-dimethylaminoethoxy)phenyl]-3-(4-phenoxyphenyl)-1,3-dihydroimidazol-2-one (50 mg) in ethanol (5 mL) under nitrogen. The nitrogen atmosphere was replaced by hydrogen and the mixture was shaken for 8 hours. The catalyst was filtered off and the filtrate was concentrated. The product with the molecular weight of 417.51 (C25H27N3O3); MS (ESI): 418 ([M+H]+), was obtained in this way.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07141561B2
Source datasetuspto-grants-2006_11
ORD IDord-5caf65059b3443d883c9831630e02d7c
Source noteuspto-grants-2006_11