HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 67136987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | (4-phenoxyphenyl)hydrazine | HCID 2760972 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67136987 | HCID 67136987 | — |
Reaction Steps
A suspension of (4-phenoxyphenyl)hydrazine (J. Org. Chem. 1956, 395; 1.5 g) in methanol (10 mL) was mixed with benzaldehyde (0.76 mL) and heated to reflux. The crystals which separated out on cooling were filtered off with suction. The product with the molecular weight of 288.35 (C19H16N2O); MS (ESI): 289 ([M+H]+), was obtained in this way.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141561B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-559485146324438eaa0a475c3a734b00 |
| Source note | uspto-grants-2006_11 |