HRID724159

反应详情

EQUATION

反应方程式

HRID 724159 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of benzyl ethyl 2-(6-nitro-3-pyridinyl)malonate (5.26 g, 15.3 mmol,) in ethanol was added palladium on carbon (530 mg) and stirred for 6 h under hydrogen atmosphere at room temperature. The catalyst was filtered off through a pad of celite and the filtrate was concentrated to give a title compound as yellow brown oil.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off through a pad of celite
  2. concentrationthe filtrate was concentrated