反应详情

To a suspension of 35 in toluene is added Lawesson's Reagent. The suspension is heated at reflux while stirring for 1 h. The reaction mixture is cooled over ice to precipitate the product. The product is then filtered, washed with hexane, and dried to give 156.

1. temperatureThe suspension is heated
2. temperatureat reflux
3. temperatureThe reaction mixture is cooled over ice
4. customto precipitate the product
5. filtrationThe product is then filtered
6. washwashed with hexane
7. customdried