Toluene → HCID 69597933, compound

Participants

Reaction Steps

A solution of 1-G (0.76 g, 1.8 mmol) in 30% TFA in CH2Cl2 (15 mL) was stirred at 25° C. for 2 h. The reaction mixture was concentrated in vacuo to give a solid. The salt was co-evaporated with toluene (2×20 mL) to yield 1-H as a tan solid (quantitative) which was used in the next step without further purification.

Provenance & Evidence