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HRID724591

反应详情

EQUATION

反应方程式

HRID 724591 的结构方程式

REACTANTS

反应物

2
结构：OCc1ccc(B(O)O)cc1
HCID2734706

4-(Hydroxymethyl)phenylboronic acid

C7H9BO3

结构：CC(C)(C)N1C(=O)C=C(Cl)S1(=O)=O
HCID21878638

2-tert-Butyl-5-chloro-1H-1lambda~6~,2-thiazole-1,1,3(2H)-trione

C7H10ClNO3S

PRODUCTS

生成物

1
结构：CC(C)(C)N1C(=O)C=C(c2ccc(CO)cc2)S1(=O)=O
HCID58746547

未命名化合物

PROCEDURE

实验过程

This compound was prepared according to the procedure of Example 1.1, Step 4, using 9-A and 4-(hydroxymethyl)phenylboronic acid as the starting materials. 1H NMR (500 MHz, CDCl3): δ 7.77 (d, J=8.3 Hz, 2H), 7.52 (d, J=8.3 Hz, 2H), 6.64 (s, 1H), 4.79 (d, J=5.9 Hz, 2H), 1.86–1.84 (m, 1H), 1.73 (s, 9H); LCMS found for C14H17NO4SNa (M+Na)+: m/z=318.

WORKUP

后处理

  1. customThis compound was prepared