反应详情

To a solution of benzylmagnesium chloride (2.0M in tetrahydrofuran, 1.32 mmol) in 5 mL of tetrahydrofuran at -78° C. under argon was added tributyltin chloride (0.36, 1.27 mmol). After 15 min, the reaction mixture was allowed to warm to room temperature. After 3 hours, solvent was removed, and the residue was purified by flash chromatography, eluting with dichloromethane/hexanes, to give 0.45 g of a clear, colorless oil.

1. waitAfter 3 hours
2. customsolvent was removed
3. customthe residue was purified by flash chromatography
4. washeluting with dichloromethane/hexanes
5. customto give 0.45 g of a clear, colorless oil