HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium hydride → HCID 178419343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium hydride | HCID 82127 | — |
| Reactant | Zirconium chloride (ZrCl4), (T-4)- | HCID 9856075 | — |
| Reactant | HCID 67593167 | HCID 67593167 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178419343 | HCID 178419343 | — |
Reaction Steps
Again the procedure of Example I was used but in this case 0.677 mmol of potassium hydride was used in place of the n-butyllithium and the starting material was 2-(para-bromophenyl) tetrahydroindene in the amount of 0.615 mmol in 8 ml of diethylether. The procedure employed 0.31 mmol of the zirconium tetrachloride. The resulting product was purified and identified as bis(2-(para-bromophenyl) tetrahydroindenyl) zirconium dichloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705579 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-4c9d8cb265bb406a993b4ab5332f3db5 |
| Source note | uspto-grants-1998_01 |