HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21847197, compound → HCID 21847179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21847197 | HCID 21847197 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21847179 | HCID 21847179 | — |
Reaction Steps
The product of Example 15 was dissolved in 700 ml of tetrahydrofuran and 2 g of palladium on activated charcoal were added. Hydrogenation (1.2 bar) was carried out for 20 hours and after filtering and evaporating the solvent, 6.9 g of the expected product were obtained which was identical to that of Stage A of Example 15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705704 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-8adc286bcfe0436883b03874f9b11642 |
| Source note | uspto-grants-1998_01 |