HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → HCID 54038932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | Methyl 4-{[(benzyloxy)carbonyl]amino}butanoate | HCID 13874704 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54038932 | HCID 54038932 | — |
Reaction Steps
5.02 g of 4-benzyloxycarbonylaminobutyric acid methyl ester are stirred under reflux in 35 ml of ethanol with 15 ml of 2-methoxyethylamine for 5 days. The reaction mixture is concentrated by evaporation and the residue is purified by means of FC (240 g of silica gel, dichloromethane/methanol=95:5). The title compound is obtained: Rf (dichloromethane/methanol=95:5)=0.33.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705658 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-40b375caf74840b78194d222ce973d69 |
| Source note | uspto-grants-1998_01 |