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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 725819Generated: October 30, 2026

HCID 15933105, compound → HCID 19709726, compound

https://huagongshe.com/reaction/725819

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15933105HCID 15933105—
ReactantHCID 178418806HCID 178418806—
SolventTolueneHCID 1140—
ProductHCID 19709726HCID 19709726—

Reaction Conditions

Temperature115 °C

Reaction Steps

A toluene solution (2.5 ml) containing 1.8 g of 3-aminopyrazole and 3 g of 2-methyl-3-oxoheptanenitrile was heated at 115° C. for 3.5 hours. Toluene was distilled off under reduced pressure and the residue was recrystallized from ethyl acetate and washed with diethyl ether to provide 2.4 g of the title object compound as colorless crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05707997
Source datasetuspto-grants-1998_01
ORD IDord-988127e807104afe8734c6e4a371fb70
Source noteuspto-grants-1998_01