Dimethylamine → HCID 19709001, compound

HRID 725843Notes

Reaction equation

HRID 725843 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]2[C:10]3[N:18]=[C:17]([N:19]4[CH2:24][CH2:23][CH:22]([C:25]([OH:27])=O)[CH2:21][CH2:20]4)[N:16]=[CH:15][C:11]=3[N:12]=[CH:13][N:14]=2)[CH:5]=[CH:6][CH:7]=1.F[B-](F)(F)F.N1(O[C:43](N(C)C)=[N+:44](C)[CH3:45])C2C=CC=CC=2N=N1.CNC>C(N(CC)CC)C>[CH3:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]2[C:10]3[N:18]=[C:17]([N:19]4[CH2:20][CH2:21][CH:22]([C:25]([N:44]([CH3:45])[CH3:43])=[O:27])[CH2:23][CH2:24]4)[N:16]=[CH:15][C:11]=3[N:12]=[CH:13][N:14]=2)[CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 674DimethylamineHCID 2733207O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborateHCID 19709094HCID 19709094, compound

Product 1

HCID 19709001HCID 19709001, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Prepared from compound 46 of Example 1 by reaction with O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate, triethylamine and dimethylamine.

Sources & evidence

ORD record
ord-f462d660dbbc4f5e97eabcae1b5a5b9d
Source dataset
uspto-grants-1998_01
Patent number
US05707989

Reaction notes

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