HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19709590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | o-Fluorobenzaldehyde | HCID 67970 | — |
| Reactant | 2-Amino-1-(morpholin-4-yl)ethan-1-one--hydrogen chloride (1/1) | HCID 12291814 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19709590 | HCID 19709590 | — |
Reaction Steps
D 4-[2-(2-Fluorobenzylidaneamino)acetyl]morpholine can be prepared as described in Example 2D, but from 5.3 cm3 of 2-fluorobenzaldehyde, 9.1 g of 4-(2-aminoacetyl)morpholine hydrochloride, 6 g of 4 Å seive and 7 cm3 of triethylamine in 150 cm3 of dichloromethane. After treatment, there are obtained 12 g of 4-[2-(2-fluorobenzylideneamino)acetyl]morpholine in the form of an oil used as is in the subsequent syntheses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05707991 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-f3079257dfc8430aa21b28126e294f43 |
| Source note | uspto-grants-1998_01 |