HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19710186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18705875 | HCID 18705875 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19710186 | HCID 19710186 | — |
Reaction Steps
A solution of 5-trifluoromethansulfonyloxy-6-hydroxy-2-(di-n-propylamino)indan (Example 7) in DMF is added to a suspension of sodium hydride in DMF under nitrogen. The mixture is alkylated with methyl iodide to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05708018 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-0f6a4f144cc54f129964afc57bd9220b |
| Source note | uspto-grants-1998_01 |