HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → HCID 19710200, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | HCID 19710195 | HCID 19710195 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19710200 | HCID 19710200 | — |
Reaction Steps
A solution of 5-carbomethoxy-6-methoxy-2-(di-n-propylamino)indan (Example 57) in THF under nitrogen is treated with DIBAL-H at -78° C. After work-up and purification, the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05708018 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-e6d3e01ac1ee4ba3bd2460859a17f53e |
| Source note | uspto-grants-1998_01 |