HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (+)- → HCID 53842783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (+)- | HCID 643189 | — |
| Reactant | Trimethylpyruvic acid amide | HCID 12922742 | — |
| Product | HCID 53842783 | HCID 53842783 | 67% |
Reaction Steps
The procedure described under n) was carried out using 5.0 g of 3,3-dimethyl-2-oxo-butyramide and 10.0 g of (R)-1-phenylethylamine. After a single crystallization from hexane there were isolated 6.0 g (67%) of (R)-3,3-dimethyl-2-(1-phenylethylimino)-butyramide of melting point 100°-101° C. [α]=+61.4 (c=0.8, CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05710322 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-d05512a1c5294de4986ce87d31476a47 |
| Source note | uspto-grants-1998_01 |