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HRID727168

反应详情

EQUATION

反应方程式

HRID 727168 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：CC1(C)Cc2cccc(CBr)c2O1
HCID4271936

7-(bromomethyl)-2,2-dimethyl-3H-1-benzofuran

C11H13BrO

PRODUCTS

生成物

1
结构：CC1(C)Cc2cccc(C[P+](c3ccccc3)(c3ccccc3)c3ccccc3)c2O1.[Br-]
HCID19705240

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

This compound is prepared in a manner analogous to that of Step A of Example 2, using 11.8 grams (0.049 mole) of 2,3-dihydro-2,2-dimethylbenzofuran-7-ylmethyl bromide and 13.0 grams (0.050 mole) of triphenylphosphine in about 100 mL of toluene, yielding (2,3-dihydro-2,2-dimethylbenzofuran-7-ylmethyl)triphenylphosphonium bromide.

WORKUP

后处理

  1. customThis compound is prepared in a manner analogous to that of Step A of Example 2