HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 19705234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Lithium Bromide | HCID 82050 | — |
| Reactant | Benzenemethanol, 3-chloro-.alpha.,.alpha.-dimethyl- | HCID 593110 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19705234 | HCID 19705234 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Step A of Example 5, using 8.5 grams (0.05 mole) of 2-(3-chlorophenyl)propan-2-ol, 8.7 grams (0.1 mole) of lithium bromide, and 13.5 grams (0.125 mole) of trimethylsilyl chloride in 100 mL of acetonitrile, yielding 2-bromo-2-(3-chlorophenyl)propane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05712281 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-b54c55974a5c42bb8a03d7cd5eecabf8 |
| Source note | uspto-grants-1998_01 |