HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22101804, compound → HCID 54365815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22101804 | HCID 22101804 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54365815 | HCID 54365815 | — |
Reaction Steps
The product from Example 53 in ethanol was shaken with 10% palladium-on-charcoal under an atmosphere of hydrogen for 3 hours. The catalyst was filtered off and the filtrate was evaporated to dryness. Flash chromatography of the residue thus obtained gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05712299 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-12379d04d2b743b880744b36cb02ec56 |
| Source note | uspto-grants-1998_01 |