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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 727762Generated: October 27, 2026

Potassium Carbonate → HCID 178444531, compound

https://huagongshe.com/reaction/727762

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant2-TrifluoroacetylphenolHCID 2761164—
ReactantHCID 178444389HCID 178444389—
SolventDimethylformamideHCID 6228—
ProductHCID 178444531HCID 178444531—

Reaction Conditions

Temperature140 °C

Reaction Steps

A mixture of 0.1 mol of trifluoroacetylphenol, 0.11 mol of trans-4-pentylcyclohexylmethyl bromide, 0.3 mol of K2CO3 and 250 ml DMF is heated at 140° C. for 10 hours. Customary work-up and crystallization give 4-(trans-4-pentylcyclohexylmethoxy)-1-trifluoroacetylbenzene, mp. 60° C., Δε=13.7.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05045229
Source datasetuspto-grants-1991_09
ORD IDord-657f9c54baf848608026045d8a1307ff
Source noteuspto-grants-1991_09