Hydroxyamine hydrochloride → HCID 54237145, compound

HRID 727826Notes

Reaction equation

HRID 727826 reaction equation
[CH3:1][N:2]([CH3:22])[S:3]([N:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([Cl:17])=[C:13]([Cl:18])[C:12]=2[Cl:19])[N:8]=[C:7]1[CH:20]=O)(=[O:5])=[O:4].Cl.[CH2:24]([O:27][NH2:28])[CH:25]=[CH2:26].Cl.NO>>[CH2:24]([O:27][N:28]=[CH:20][C:7]1[N:6]([S:3](=[O:5])(=[O:4])[N:2]([CH3:22])[CH3:1])[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([Cl:17])=[C:13]([Cl:18])[C:12]=2[Cl:19])[N:8]=1)[CH:25]=[CH2:26]

Participants

4

Reactant 3

HCID 443297Hydroxyamine hydrochlorideHCID 3084724O-Allylhydroxylamine hydrochlorideHCID 19825126HCID 19825126, compound

Product 1

HCID 54237145HCID 54237145, compound

Procedure

1-(Dimethylsulphamoyl)-2-formyl-4-(2,3,4-trichlorophenyl)imidazole was reacted with O-allylhydroxylamine hydrochloride in a similar manner to the reaction with hydroxylamine hydrochloride described in Example 1, to give 2-allyloxyiminomethyl-1-(dimethylsulphamoyl)-4-(2,3,4-trichlorophenyl)imidazole, m.p. 87°-88°. (Compound 9)

Sources & evidence

ORD record
ord-13158f72f911485aba227747d77f57e1
Source dataset
uspto-grants-1991_09
Patent number
US05045557

Reaction notes

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