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HRID727829

反应详情

EQUATION

反应方程式

HRID 727829 的结构方程式

REACTANTS

反应物

4
结构：CN(C)S(=O)(=O)Cl
HCID83372

Dimethylsulphamoyl chloride

C2H6ClNO2S

结构：CCOC(=O)c1nc[nH]c1C
HCID99200

Ethyl 4-methylimidazole-5-carboxylate

C7H10N2O2

结构：CCOC(c1ccccc1)(c1ccccc1)c1nc[nH]c1C
HCID19825136

未命名化合物

结构：Br[Mg]c1ccccc1
HCID178418255

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(c1ccccc1)(c1ccccc1)c1ncn(S(=O)(=O)N(C)C)c1C
HCID19825131

4-[Ethoxy(diphenyl)methyl]-N,N,5-trimethyl-1H-imidazole-1-sulfonamide

C21H25N3O3S

PROCEDURE

实验过程

Ethyl 5-methylimidazole-4-carboxylate was converted by a Grignard reaction, using phenylmagnesium bromide, to 4-[ethoxy(diphenyl)methyl]-5-methylimidazole, m.p. 205°. This was then treated with dimethylsulphamoyl chloride in a similar manner to that described in Example 1, to give 1-dimethylsulphamoyl-4-[ethoxy(diphenyl)methyl)-5-methylimidazole, m.p. 150°.