HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-[1-(1-Imidazolyl)-butyl]-benzoic acid, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-[1-(1-Imidazolyl)-butyl]-benzoic acid | HCID 14514368 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-[1-(1-Imidazolyl)-butyl]-benzoic acid, hydrochloride | HCID 14514369 | — |
Reaction Steps
1.0 g of 4-[1-(1-imidazolyl)-butyl]-benzoic acid is dissolved in 20 ml of ethanol and mixed with 10 ml of concentrated hydrochloric acid. The reaction mixture is precipitated into 100 ml of water and the precipitate is suctioned off. After recrystallization from ethanol, 0.95 g of 4-[1-(1-imidazolyl)-butyl]-benzoic acid, hydrochloride with a melting point of 38° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05045558 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-fc283fd46dc345c19663bdc84467f22e |
| Source note | uspto-grants-1991_09 |