HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanate → HCID 15171496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Reactant | HCID 10422999 | HCID 10422999 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15171496 | HCID 15171496 | — |
Reaction Steps
A mixture of 2-[2-(4-aminophenyl)ethyl]-3,7-dimethylimidazo[1,2-a]pyridine (2.2 g) and ethyl isothiocyanate (0.8 ml) in ethanol (20 ml) was refluxed for 1.5 hours. The solvent was evaporated and the residue was triturated with diethyl ether. The precipitate was collected by filtration and dried to give 3,7-dimethyl-2-[2-{4-(3-ethylthioureido)phenyl}ethyl]imidazo[1,2-a]pyridine (2.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047411 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-3767f4a68bf547ffa9e1e3c8f816d8b1 |
| Source note | uspto-grants-1991_09 |