HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 15171530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 10083053 | HCID 10083053 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15171530 | HCID 15171530 | — |
Reaction Steps
A solution of 6-[(2-pyridyl)methyl]-2-aminobenzothiazole (1.3 g) and ethyl isocyanate (0.6 ml) in tetrahydrofuran (25 ml) was stirred at 60° C. for 4 hours. Evaporation of the solvent gave a residue which was crystallized from tetrahydrofuran. The crystal was collected by filtration to give 6-[(2-pyridyl)methyl]-2-(3-ethylureido)benzothiazole (0.68 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047411 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-7fb4448cff0c49b6a34850e241827bf0 |
| Source note | uspto-grants-1991_09 |