HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178436741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178436742 | HCID 178436742 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178436741 | HCID 178436741 | — |
Reaction Steps
A solution of 3-(4-Boc-piperazin-1-yl)-1-ethyl-9-methyl-7-morpholinophenothiazin-5-ium iodide (65 mg, 0.01 mmol) in dichloromethane (10 mL) and trifluoroacetic acid (1.0 mL) was stirred for 1 h at 50° C. The resulting mixture was washed by toluene (2×5 mL), pentane (2×5 mL) and concentrated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08828986B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-df671367bca54720b6beb02e1c0edada |
| Source note | uspto-grants-2014_09 |