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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 72819Generated: October 30, 2026

Trifluoroacetic acid → HCID 178436741, compound

https://huagongshe.com/reaction/72819

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 178436742HCID 178436742—
SolventDichloromethaneHCID 6344—
ProductHCID 178436741HCID 178436741—

Reaction Steps

A solution of 3-(4-Boc-piperazin-1-yl)-1-ethyl-9-methyl-7-morpholinophenothiazin-5-ium iodide (65 mg, 0.01 mmol) in dichloromethane (10 mL) and trifluoroacetic acid (1.0 mL) was stirred for 1 h at 50° C. The resulting mixture was washed by toluene (2×5 mL), pentane (2×5 mL) and concentrated to dryness.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08828986B2
Source datasetuspto-grants-2014_09
ORD IDord-df671367bca54720b6beb02e1c0edada
Source noteuspto-grants-2014_09