HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 53634746, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 53910051 | HCID 53910051 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53634746 | HCID 53634746 | 48.6% |
Reaction Steps
A mixture of 4-[2-(4-acetamido-3-nitrophenyl)vinyl]-5-methyl-1-tritylimidazole (6.3 g) in ethanol (60 ml) and 1N-sodium hydroxide (23.8 ml) was refluxed for 1 hour and the mixture was cooled. The isolated precipitate was collected by filtration and the precipitate was washed with aqueous ethanol to give 4-[2-(4-amino-3-nitrophenyl)vinyl]-5-methyl-1-tritylimidazole (2.82 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047411 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-a078c8d164ce4716bcd99b67fe9c0f5b |
| Source note | uspto-grants-1991_09 |