Dichloromethane → HCID 178436735, compound

Participants

Reaction Steps

A solution of 1-ethyl-9-methyl-7-morpholino-3-(4-Boc-1,4-diazepane-1-yl)phenothiazin-5-ium iodide (65 mg, 0.1 mmol) in dichloromethane (10 mL) and HCl (1.0 mL, 4 M solution in 1,4-dioxane) was stirred for 2 h at 50° C. Product was precipitated, liquid was decanted. Solid material was dissolved in methanol and concentrated to dryness.

Provenance & Evidence