反应详情

A solution of 1-ethyl-9-methyl-7-morpholino-3-(4-Boc-1,4-diazepane-1-yl)phenothiazin-5-ium iodide (65 mg, 0.1 mmol) in dichloromethane (10 mL) and HCl (1.0 mL, 4 M solution in 1,4-dioxane) was stirred for 2 h at 50° C. Product was precipitated, liquid was decanted. Solid material was dissolved in methanol and concentrated to dryness.

1. customProduct was precipitated
2. customliquid was decanted
3. dissolutionSolid material was dissolved in methanol
4. concentrationconcentrated to dryness