HuagongsheHuagongshe Chemistry Print Report · For research reference only
12-Aminododecanoic Acid → HCID 19824103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 12-Aminododecanoic Acid | HCID 69661 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19824103 | HCID 19824103 | 110.4% |
Reaction Steps
Reaction similar to example 2, of 9.30 g (50.0 mmol) N-hydroxysuccinimide and 12.0 g (58.0 mmol) DCC gave 14.0 g (100%) of the succinimidylester, which was reacted with 12.5 g (58.1 mmol) 12-aminododecanoic acid to yield 12.3 g (65%) colourless crystals, m.p. 102°-104° C. (methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047535 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-f9d2fbab8a39468b8883567d49bd7737 |
| Source note | uspto-grants-1991_09 |