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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 72827Generated: October 30, 2026

Dichloromethane → HCID 178505950, compound

https://huagongshe.com/reaction/72827

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 70895770HCID 70895770—
ProductHCID 178505950HCID 178505950—

Reaction Conditions

Temperature40 °C

Reaction Steps

To a solution 3-morpholino-7-(pyrrolidin-1-yl)-1-fluoro-10-Boc-phenothiazine (150 mg) in dichloromethane (10 mL) HCl (2 mL, 4 M solution in 1,4-dioxane)) was added. The reaction mixture was stirred at 40° C. for 3 h. Solvent was removed under vacuum. Product was purified by flash chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08828986B2
Source datasetuspto-grants-2014_09
ORD IDord-98aba1761eca447791d9603b8ca1fd4f
Source noteuspto-grants-2014_09