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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 72830Generated: October 30, 2026

Dichloromethane → HCID 178482910, compound

https://huagongshe.com/reaction/72830

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 70895830HCID 70895830—
ProductHCID 178482910HCID 178482910—

Reaction Conditions

Temperature40 °C

Reaction Steps

To a solution 3-dimethylamino-7-morpholino-1-fluoro-10-Boc-phenothiazine (15) (100 mg) in dichloromethane (10 mL) HCl (1 mL, 4 M solution in 1,4-dioxane)) was added. The reaction mixture was stirred at 40° C. for 3 h. Solvent was removed under vacuum. Product was purified by flash chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08828986B2
Source datasetuspto-grants-2014_09
ORD IDord-e9bdc129581e4f1189be83baf8ed3d7a
Source noteuspto-grants-2014_09