HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 54143333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 1,1-Dimethylhydrazine | HCID 5976 | — |
| Reactant | 1-[1-(4-Chlorophenyl)cyclobutyl]ethanone | HCID 21258408 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54143333 | HCID 54143333 | — |
Reaction Steps
A mixture of 1-[1-(4-chlorophenyl)cyclobutyl]-ethanone (40 g), N,N-dimethylhydrazine (50 ml), glacial acetic acid (2 ml) and ethanol (35 ml) was heated under reflux for 78 hours. Removal of the solvent gave a residue which was distilled (104°-106°/0.1 mm Hg) to give 1-[1-(4-chlorophenyl)cyclobutyl]ethanone N,N-dimethylhydrazone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047432 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-2570d4cf24f7454ab91ce74567d8807e |
| Source note | uspto-grants-1991_09 |