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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 72833Generated: October 30, 2026

Dichloromethane → HCID 178505949, compound

https://huagongshe.com/reaction/72833

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 70895826HCID 70895826—
ProductHCID 178505949HCID 178505949—

Reaction Conditions

Temperature40 °C

Reaction Steps

To a solution 3-(4-Boc-1,4-diazepan-1-yl)-7-morpholino-1-fluoro-10-Boc-phenothiazine (0.8 g) in dichloromethane (10 mL) HCl (2 mL, 4 M solution in 1,4-dioxane)) was added. The reaction mixture was stirred at 40° C. for 3 h. Solvent was removed under vacuum. Product was purified by flash chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08828986B2
Source datasetuspto-grants-2014_09
ORD IDord-799ca0ef64124ef091dc3153921a7fe3
Source noteuspto-grants-2014_09