HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 72833Generated: October 30, 2026
Dichloromethane → HCID 178505949, compound
https://huagongshe.com/reaction/72833
Participants
| Role | Name | HCID | Charge |
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| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 70895826 | HCID 70895826 | — |
| Product | HCID 178505949 | HCID 178505949 | — |
Reaction Steps
To a solution 3-(4-Boc-1,4-diazepan-1-yl)-7-morpholino-1-fluoro-10-Boc-phenothiazine (0.8 g) in dichloromethane (10 mL) HCl (2 mL, 4 M solution in 1,4-dioxane)) was added. The reaction mixture was stirred at 40° C. for 3 h. Solvent was removed under vacuum. Product was purified by flash chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08828986B2 |
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| Source dataset | uspto-grants-2014_09 |
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| ORD ID | ord-799ca0ef64124ef091dc3153921a7fe3 |
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| Source note | uspto-grants-2014_09 |
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