HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Sulfate → HCID 15028916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Sulfate | HCID 6163 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178499159 | HCID 178499159 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15028916 | HCID 15028916 | — |
Reaction Steps
The intermediate was prepared according to process SCHEME I of EXAMPLE 1c by reacting 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-methoxycarbonyl-4-trifluoromethylsulfenyl-5-hydroxypyrazole with diethyl sulfate and sodium hydride in dioxane. The following spectral data were obtained: MS, m/e=482(M+); NMR (CDCl3) δ1.43 (t, J=7.0 Hz, C2H5), 3.73 (s, OCH3), 4.4 (q, J=7.0, OCH2), and 7.76 (s, 2H aromatic).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047550 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-c952d5c63d5f4f3183b372b093031955 |
| Source note | uspto-grants-1991_09 |