Phthalimide → 3-Hexadecylthio-2-methoxymethylpropylamine

HRID 728479Notes

Reaction equation

HRID 728479 reaction equation
[CH2:1]([S:17][CH2:18][CH:19]([CH2:22][O:23][CH3:24])[CH2:20]O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].ClCCCS([NH:32]CC(OC)CSCCCCCCCCCCCCCCCC)(=O)=O.C1(=O)NC(=O)C2=CC=CC=C12>>[CH2:1]([S:17][CH2:18][CH:19]([CH2:22][O:23][CH3:24])[CH2:20][NH2:32])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 3

HCID 6809PhthalimideHCID 109812793-Hexadecylthio-2-methoxymethylpropanolHCID 14835022HCID 14835022, compound

Product 1

HCID 148350103-Hexadecylthio-2-methoxymethylpropylamine

Procedure

3-Hexadecylthio-2-methoxymethylpropanol IVk3 is allowed to react and worked up by the same procedure as described in (4). The phthalimide compound m.p. 45° C. The summary of the experimental condition and the physical data of the product are listed in Tables 5 and 6.

Workup

  1. customto react

Sources & evidence

ORD record
ord-5354b8926c48468b8b73c6312c0d10be
Source dataset
uspto-grants-1991_09
Patent number
US05047540

Reaction notes

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