HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Benzoyloxypropan-1-yl)-3-octadecylcarbamoyloxypropylamine → 2-Cyanomethyl-3-octadecylcarbamoyloxypropylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Benzoyloxypropan-1-yl)-3-octadecylcarbamoyloxypropylamine | HCID 14835012 | — |
| Reactant | 1-Azido-2-cyanomethyl-3-octadecylcarbamoyloxypropane | HCID 54434095 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Cyanomethyl-3-octadecylcarbamoyloxypropylamine | HCID 14835014 | — |
Reaction Steps
A mixture of 1-azido-2-cyanomethyl-3-octadecylcarbamoyloxypropane Vn2b, 80 mg of 10% palladium on charcoal in 40 ml of methanol is hydrogenated by the same procedure as described in (129) and crude product of the titled compound IVn2 is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047540 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-4b70a0b57e6940cdbea92491340a5218 |
| Source note | uspto-grants-1991_09 |