HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 54543603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzoylhydrazine | HCID 11955 | — |
| Reactant | 2,4-Dimethyl-5-acetylthiazole | HCID 520888 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54543603 | HCID 54543603 | 54% |
Reaction Steps
A mixture of 5.0 gm (0.322 mole) of 5-acetyl-2,4-dimethylthiazole, 4.38 gm (0 0322 mole) of benzhydrazide, 10 drops of glacial acid and 100 ml of ethanol is refluxed 48 hrs. The reaction mixture is diluted with water to the cloud point then chilled. The product is collected and dried to give 4.75 gm (54%) of the title compound having a melting point of 138.4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05049561 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-789d7cef10b748cabac080fbbade07d0 |
| Source note | uspto-grants-1991_09 |