4-Cyanobenzoic acid → HCID 15044879, compound

HRID 728565Notes

Reaction equation

HRID 728565 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([C:8]([CH3:11])([CH3:10])[CH3:9])[C:5]([OH:12])=[C:4]([C:13]([CH3:16])([CH3:15])[CH3:14])[CH:3]=1.[C:17]([C:19]1[CH:27]=[CH:26][C:22]([C:23](O)=[O:24])=[CH:21][CH:20]=1)#[N:18]>>[C:17]([C:19]1[CH:27]=[CH:26][C:22]([C:23]([NH:1][C:2]2[CH:3]=[C:4]([C:13]([CH3:16])([CH3:15])[CH3:14])[C:5]([OH:12])=[C:6]([C:8]([CH3:9])([CH3:10])[CH3:11])[CH:7]=2)=[O:24])=[CH:21][CH:20]=1)#[N:18]

Participants

3

Reactant 2

HCID 120874-Cyanobenzoic acidHCID 3142204-Amino-2,6-di-tert-butylphenol

Product 1

HCID 15044879HCID 15044879, compoundYield 50.2%

Procedure

Using the method of Example 12, 3.4 g of 4-amino-2,6-di-t-butylphenol was reacted with 2.3 g of 4-cyanobenzoic acid to provide 2.7 g of 4-cyano-N-(3',5'-di-t-butyl-4'-hydroxyphenyl)benzamide.

Sources & evidence

ORD record
ord-492ad44a69d24e1b9c27f18d419d7f0f
Source dataset
uspto-grants-1991_09
Patent number
US05049572

Reaction notes

Loading…