HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylbutylamine → HCID 54165061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylbutylamine | HCID 8068 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54165061 | HCID 54165061 | — |
Reaction Steps
A solution of 8.26 g (0.05 mol) of 1-nitro-2,2-di(methylthio)ethylene and 5.25 g (0.06 mol) of N-n-butyl-N-methylamine in toluene is refluxed for 2 hours. After evaporation of the toluene under vacuum, 10.2 g of 2-(N-butyl-N-methylamino)-2-methylthio-1-nitroethylene are isolated as an oil (nD21 =1.584). (Compound 2.1, Table 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05049571 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-fd3bc811432a448ea31989fc409fd280 |
| Source note | uspto-grants-1991_09 |