Salicylaldehyde → HCID 54017688, compound

HRID 728777Notes

Reaction equation

HRID 728777 reaction equation
[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[CH2:12]2.[OH:19][C:20]1[CH:27]=[CH:26][CH:25]=[CH:24][C:21]=1[CH:22]=O>>[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[CH:22][C:21]1[CH:24]=[CH:25][CH:26]=[CH:27][C:20]=1[OH:19]

Participants

3

Reactant 2

HCID 6998SalicylaldehydeHCID 13689754HCID 13689754, compound

Product 1

HCID 54017688HCID 54017688, compoundYield 62%

Procedure

Starting from 5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-1,3-dihydro-2H-indol-2-one and 2-hydroxy benzaldehyde and following the method described in Example 10, the desired compound was obtained.

Sources & evidence

ORD record
ord-6173304025b041cbbdf64050eb154fb6
Source dataset
uspto-grants-1991_09
Patent number
US05051417

Reaction notes

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