3-Pyridinecarboxaldehyde → HCID 54210936, compound

HRID 728778Notes

Reaction equation

HRID 728778 reaction equation
[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[CH2:12]2.[N:19]1[CH:24]=[CH:23][CH:22]=[C:21]([CH:25]=O)[CH:20]=1>>[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[CH:25][C:21]1[CH:20]=[N:19][CH:24]=[CH:23][CH:22]=1

Participants

3

Reactant 2

HCID 103713-PyridinecarboxaldehydeHCID 13689754HCID 13689754, compound

Product 1

HCID 54210936HCID 54210936, compoundYield 75%

Procedure

Starting from 5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-1,3-dihydro-2H-indol-2-one and pyridine 3-carboxaldehyde and following the method described in Example 10, the desired compound was obtained.

Sources & evidence

ORD record
ord-ca4528195200444e8dbaf9dd8681d817
Source dataset
uspto-grants-1991_09
Patent number
US05051417

Reaction notes

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