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HRID728824

反应详情

EQUATION

反应方程式

HRID 728824 的结构方程式

REACTANTS

反应物

4
结构：CO
HCID887

Methanol

CH4O

结构：O
HCID962

Water

H2O

结构：c1ccc(OCC2CO2)cc1
HCID31217

Phenyl glycidyl ether

C9H10O2

结构：CS(=O)(=O)Nc1ccc(CN)cc1.Cl
HCID2760996

4-(Methylsulfonylamino)benzylamine hydrochloride

C8H13ClN2O2S

PRODUCTS

生成物

1
结构：Cc1cccc(OCC(O)CNCc2ccc(NS(C)(=O)=O)cc2)c1.Cl
HCID67689925

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[K+].[OH-]
溶剂HCID14797

Potassium hydroxide

HKO

PROCEDURE

实验过程

Heat a mixture of N-[4-(aminomethyl)phenyl]methanesulfonamide hydrochloride(15.0 g, 63.4 mmol) and 1,2-epoxy-3-phenoxypropane (10.41 g, 63.4 mmol) in 63.4 mL of 1 N KOH in methanol and 10 mL of water for about 3.5 h. Remove the solvent to afford crystals of the title compound.

WORKUP

后处理

  1. temperatureHeat
  2. customRemove the solvent