HRID728827

反应详情

EQUATION

反应方程式

HRID 728827 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 2.39 g (13.2 mmol) 1,2-epoxy-3-(4-methoxyphenoxy)propane in 25 mL methanol is added 3.05 g (13.2 g) N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide. The reaction mixture is stirred under a nitrogen atmosphere for 24 h. After this time, the precipitate is collected and recrystallized from ethanol to provide the title compound.

WORKUP

后处理

  1. customAfter this time, the precipitate is collected
  2. customrecrystallized from ethanol